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First, dilution of L-carnitine, content to 1 000 mg/kg or less than 1 000 mg/kg, and then extract it according to the method in 7.1.1 7.1.3 Solid beverage category, Weigh the appropriate amount of the sample, dissolve and dilute it with water to make the content of L-carnitine less than or equal to 1000 mg/kg, then extract it according to the method in 7.1.1 7.2 Purification Take 1 mL of the solution in an activated cationic solid phase extraction column (4.18), the rate of 1 drop/sec column, with 3 mL 10 mmol/L aqueous solution of hydrochloric acid (4.15), discard those solutions, vacuum for 1min, place 2 mL 4% ammonium methanol solution into the syringe(4.17), collect the elution into a 15- mL conical tube, Dry with nitrogen evaporator at 40