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The crude material was purified by Isolera flash column chromatography on silica via gradient elution, from 100% dichloromethane to 15% methanol in dichloromethane to produce CAM-S-CAM- d 15 TPP (9.1 mg, 27%) as a pale yellow fluffy/foamy solid

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[9] That mixed result is worth stating rather than smoothing over, because it illustrates a real feature of the preclinical record: effects vary by model, species, formulation, and readout, and the literature is not a monotone chorus of positive findings

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