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1H NMR (DMSO-d 6 ,400MHz)12.88(br1H)7.78(s1H)7.41(m1H)6.91(m 2H)6.81(m2H)6.73(m2H)6.23(s1H)4.98(s2H)4.56(s 2H)3.68(s3H)ppm.MS344(MH + ) Example 1.4: synthesis of precursor 2- (4-methoxyphenoxy) -1- (3- ((thien-2-ylmethyl) amino) -1H-pyrazol-1-yl) ethanone